Cover E DIN EN IEC 62321-3-4 VDE 0042-1-3-4:2023-01
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E DIN EN IEC 62321-3-4 VDE 0042-1-3-4:2023-01

Determination of certain substances in electrotechnical products

Part 3-4: Screening of Phthalates in polymers of electrotechnical products by high performance liquid chromatography with ultraviolet detector (HPLC-UV), thin layer chromatography (TLC) and thermal desorption mass spectrometry (TD-MS)

(IEC 111/657/CDV:2022); German and English version prEN IEC 62321-3-4:2022
Class/Status: Draft, valid
Released: 2023 -01   Published: 2022-12 -16
VDE Art. No.: 1090075
End of objection deadline: 2023-02-16

This part of IEC 62321 specifies procedures for the screening of di-isobutyl phthalate (DIBP), di-n-butyl phthalate (DBP), benzyl butyl phthalate (BBP), di-(2-ethylhexyl) phthalate (DEHP) in polymers of electrotechnical products by using high performance liquid chromatography with ultraviolet detector (HPLC-UV), thin layer chromatography (TLC) and thermal desorption mass spectrometry (TD-MS).
These test methods have been evaluated by testing PE (polyethylene), PVC (polyvinyl chloride) materials containing individual phthalates between 500 mg/kg to 3 000 mg/kg as depicted in the normative and informative parts of this document. The use of the methods described in this document for other polymer types, phthalate compounds or concentration ranges other than those specified above has not been specifically evaluated.
High performance liquid chromatography with ultraviolet detector (HPLC-UV), thin layer chromatography (TLC) and thermal desorption mass spectrometry (TD-MS) techniques are described in the normative part of this document. Fourier transform infrared spectroscopy (FT-IR) is described in the informative Annex of this document.